HuagongsheHuagongshe Chemistry Print Report · For research reference only
Myristanilide → HCID 24821533, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Myristanilide | HCID 69324 | — |
| Reactant | 4-Chloro-3-nitropyridine | HCID 2735781 | — |
| Product | HCID 24821533 | HCID 24821533 | 34% |
Reaction Steps
Method B applied to 4-chloro-3-nitropyridine (79 mg, 0.5 mmol) and tetradecanoic acid phenylamide (182 mg, 0.6 mmol) afforded the title compound as viscous oil (64 mg, 34%). 1H NMR (DMSO) δ 0.83 (t, J=6.7Hz, 3H), 1.16-1.32 (m, 20H), 1.73 (p, J=6.7 Hz, 2H), 2.83 (t, J=6.7Hz, 2H). 7.63-7.71 (m, 6H), 8.56 (d, J=5.2Hz, 1H), 9.43 (s, 1H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08188282B2 |
| Source dataset | uspto-grants-2012_05 |
| ORD ID | ord-38884b08f0d7414a8361e4cf1cb35dd3 |
| Source note | uspto-grants-2012_05 |