HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-(4-Methoxyphenyl)Acetamide → HCID 24821600, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-(4-Methoxyphenyl)Acetamide | HCID 5827 | — |
| Reactant | 4-Chloro-3-nitropyridine | HCID 2735781 | — |
| Product | HCID 24821600 | HCID 24821600 | 70.2% |
Reaction Steps
Method B applied to 4-chloro-3-nitropyridine (79 mg, 0.5 mmol) and N-(4-methoxyphenyl)acetamide (99 mg, 0.6 mmol) afforded the title compound as viscous oil (84 mg, 70%). 1H NMR (DMSO) δ 2.55 (s, 3H), 3.88 (s, 3H), 7.21 (d, J=8.8Hz, 2H), 7.57 (d, J=8.8Hz, 2H), 7.69 (d, J=5.4Hz, 1H), 8.57 (d, J=5.4Hz, 1H), 9.44 (s, 1H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08188282B2 |
| Source dataset | uspto-grants-2012_05 |
| ORD ID | ord-402a5a996f714541a5c24c984f063d4e |
| Source note | uspto-grants-2012_05 |