HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetyl chloride → HCID 18613788, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetyl chloride | HCID 6367 | — |
| Reactant | 2-(4-Chlorophenyl)ethylamine | HCID 67430 | — |
| Product | HCID 18613788 | HCID 18613788 | — |
Reaction Steps
In accordance with the same procedures as in Steps 1, 2, and 3 of Preparation 21, except for using 4-chlorophenethylamine and acetyl chloride, 7-chloro-1-methyl-1,2,3,4-tetrahydroisoquinoline was obtained. In accordance with the same procedures as in Preparation 20, the titled compound was obtained as pale yellow oil. (Yield: 67%) The product was used in the subsequent step without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08188114B2 |
| Source dataset | uspto-grants-2012_05 |
| ORD ID | ord-475161a1d9c449d988b83a46df4d3b1c |
| Source note | uspto-grants-2012_05 |