HCID 86615251, compound → HCID 86615252, compound

Participants

Reaction Steps

A solution of N-(2-chloropyridin-3-yl)-N'-(1-ethylpropylidene)-hydrazine (1.3 g, 6.1 mmol) prepared in Step 2 in diphenyl ether was stirred for 3 hours at 300° C. The reaction mixture was cooled to room temperature and then purified with silica gel column chromatography to give 850 mg of the titled compound as a pale yellow solid. (Yield: 72%).

Provenance & Evidence