HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 11666949, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 11572801 | HCID 11572801 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 11666949 | HCID 11666949 | 90% |
Reaction Steps
A solution of 7-(4-chlorophenoxymethyl)-2,3-dimethyl-1H-pyrrolo[2,3-c]pyridine prepared in Example 41 in ethyl acetate (10 ml) was saturated with hydrochloric acid gas and then filtered. The resulting solid was dried under reduced pressure to give the titled compound as a white solid. (Yield: 90%)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08188114B2 |
| Source dataset | uspto-grants-2012_05 |
| ORD ID | ord-712b43200186494ca7a291d4297e46b2 |
| Source note | uspto-grants-2012_05 |