HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 67142110, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 67142111 | HCID 67142111 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 67142110 | HCID 67142110 | 90% |
Reaction Steps
A solution of 1-allyl-7-(3,4-dihydro-1H-isoquinolin-2-yl)-2,3-dimethyl-N-(4-methylbenzyl)-1H-pyrrolo[2,3-c]pyridin-5-carboxamide prepared in Step 1 in ethyl acetate was saturated with hydrochloric acid gas and then filtered to give the titled compound as a white solid. (Yield: 90%)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08188114B2 |
| Source dataset | uspto-grants-2012_05 |
| ORD ID | ord-1a5ba6a5a71e43c59d4826532be03044 |
| Source note | uspto-grants-2012_05 |