HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl 3-[4-(4-nitrophenoxy)phenyl]propionate → HCID 68523825, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl 3-[4-(4-nitrophenoxy)phenyl]propionate | HCID 68524232 | — |
| Catalyst | HCID 178418390 | HCID 178418390 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 68523825 | HCID 68523825 | — |
Reaction Steps
To a suspension of 5% palladium-carbon (0.50 g) in ethanol (50 mL) was added ethyl 3-[4-(4-nitrophenoxy)phenyl]propionate (5.00 g, 15.9 mmol), and the resulting solution was subjected to catalytic reduction at atmospheric pressure and at room temperature. Once the absorption of hydrogen had stopped, the catalyst was removed by filtration, and the filtrate was concentrated under reduced pressure, to thereby yield 4.52 g of the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08188277B2 |
| Source dataset | uspto-grants-2012_05 |
| ORD ID | ord-320e125b223041b799f4d38f39c92b39 |
| Source note | uspto-grants-2012_05 |