HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 18738154, compound → HCID 18738153, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 18738154 | HCID 18738154 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 18738153 | HCID 18738153 | 79.3% |
Reaction Steps
A mixture of ethyl 3-azido-2(S)-(benzoylamino)propionate (0.35 g) and 10% Pd—C (0.07 g) in ethanol (4 ml) was hydrogenated at an atmospheric pressure for 2 hours. After the catalyst was removed by filtration, the filtrate was concentrated in vacuo to give ethyl 3-amino-2(S)-(benzoylamino)propionate (0.25 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06384028B1 |
| Source dataset | uspto-grants-2002_05 |
| ORD ID | ord-30c5cb2d7f9c42d28be00c0e8709f04b |
| Source note | uspto-grants-2002_05 |