HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzenesulfonyl chloride → N-(3-Hydroxypropyl)benzenesulfonamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzenesulfonyl chloride | HCID 7369 | — |
| Reactant | 3-Amino-1-propanol | HCID 9086 | — |
| Product | N-(3-Hydroxypropyl)benzenesulfonamide | HCID 11333383 | 99.5% |
Reaction Steps
The preparation is carried out as in Example 1(a) from 353 g of benzenesulphonyl chloride (2 mol) and 157.7 g of 3-amino-1-propanol (2.1 mol). The amount obtained is 406.7 g, i.e. a yield of 99.5%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06384115B1 |
| Source dataset | uspto-grants-2002_05 |
| ORD ID | ord-0e7c1d38ddb44b9f99813a23edd64106 |
| Source note | uspto-grants-2002_05 |