HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethylene Glycol → HCID 86584105, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethylene Glycol | HCID 174 | — |
| Reactant | Sodium | HCID 5360545 | — |
| Reactant | Sodium chloroacetate | HCID 23665759 | — |
| Product | HCID 86584105 | HCID 86584105 | — |
Reaction Steps
To 650 g of ethylene glycol, 210.2 g (2.50 mol) of the monosodium salt of ethylene glycol obtained by the operation described above in (1) was added with stirring and dissolved at 70 to 80° C. Then, 285.5 g (2.45 mol) of sodium monochloroacetate was charged over 1 hour at the same temperature and then stirred at the same temperature for 2 hours to obtain 1145.0 g of sodium β-hydroxyethoxy acetate solution in ethylene glycol.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06384241B2 |
| Source dataset | uspto-grants-2002_05 |
| ORD ID | ord-4734ed1fbe4049db8d11b6f6b1bc24a7 |
| Source note | uspto-grants-2002_05 |