Ethylene Glycol → HCID 86584105, compound

HRID 1934850Notes

Reaction equation

HRID 1934850 reaction equation
[Na:1].Cl[CH2:3][C:4]([O-:6])=[O:5].[Na+].[CH2:8]([OH:11])[CH2:9][OH:10]>>[C:4]([O:6][O:10][CH2:9][CH2:8][OH:11])(=[O:5])[CH3:3].[Na:1]

Participants

4

Reactant 3

HCID 174Ethylene Glycol3×HCID 5360545SodiumHCID 23665759Sodium chloroacetate

Product 1

HCID 86584105HCID 86584105, compound

Procedure

To 650 g of ethylene glycol, 210.2 g (2.50 mol) of the monosodium salt of ethylene glycol obtained by the operation described above in (1) was added with stirring and dissolved at 70 to 80° C. Then, 285.5 g (2.45 mol) of sodium monochloroacetate was charged over 1 hour at the same temperature and then stirred at the same temperature for 2 hours to obtain 1145.0 g of sodium β-hydroxyethoxy acetate solution in ethylene glycol.

Workup

  1. additionwas added
  2. dissolutiondissolved at 70 to 80° C
  3. stirringstirred at the same temperature for 2 hours

Sources & evidence

ORD record
ord-4734ed1fbe4049db8d11b6f6b1bc24a7
Source dataset
uspto-grants-2002_05
Patent number
US06384241B2

Reaction notes

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