HRID1934857

反应详情

EQUATION

反应方程式

HRID 1934857 的结构方程式

REACTANTS

反应物

1

PRODUCTS

生成物

1

AUXILIARIES

试剂、催化剂与溶剂

1

CONDITIONS

反应条件

温度
190 °C

PROCEDURE

实验过程

To 680.0 grams of meadowfoam acid is added to the sorbitol intermediate. Next add 0.1% stannous oxylate based upon the total weight of the batch after all ingredients have been charged, under agitation. The temperature of the mass is raised to 180-200° C. and water is stripped off as formed. The acid value and hydroxyl value drop to vanishingly small values, and the saponification value increases to theoretical.

WORKUP

后处理

  1. additionhave been charged, under agitation
  2. customas formed
  3. temperaturethe saponification value increases to theoretical