HCID 22466735, compound → HCID 22466604, compound

HRID 1935142Notes

Reaction equation

HRID 1935142 reaction equation
[OH:1][C:2]1[CH:3]=[C:4]([NH:10][C:11]2[C:20]3[C:15](=[C:16]([O:24][CH3:25])[CH:17]=[C:18]([N+:21]([O-])=O)[CH:19]=3)[N:14]=[CH:13][C:12]=2[C:26]#[N:27])[CH:5]=[CH:6][C:7]=1[O:8][CH3:9]>[Fe]>[NH2:21][C:18]1[CH:19]=[C:20]2[C:15](=[C:16]([O:24][CH3:25])[CH:17]=1)[N:14]=[CH:13][C:12]([C:26]#[N:27])=[C:11]2[NH:10][C:4]1[CH:5]=[CH:6][C:7]([O:8][CH3:9])=[C:2]([OH:1])[CH:3]=1

Participants

3

Reactant 1

HCID 22466735HCID 22466735, compound

Product 1

HCID 22466604HCID 22466604, compound

Reagents, catalysts & solvents 1

HCID 23925IronCatalyst

Procedure

Using the method described in Example 196, 0.1 g of 4-(3-hydroxy-4-methoxy-phenylamino)-8-methoxy-6-nitro-quinoline-3-carbonitrile and 0.09 g of iron was converted to the title compound: MP=215° C. (dec)

Sources & evidence

ORD record
ord-8534e7c964f942e08de0e75d646db473
Source dataset
uspto-grants-2002_05
Patent number
US06384051B1

Reaction notes

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