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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1935403Generated: October 30, 2026

HCID 10594703, compound → HCID 15391002, compound

https://huagongshe.com/reaction/1935403

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 10594703HCID 10594703—
SolventEthyl AcetateHCID 8857—
ProductHCID 15391002HCID 15391002—

Reaction Conditions

Temperature0 °C

Reaction Steps

A solution of the product from Step D (0.570 g, 1.58 mmol) in ethyl acetate (50 mL) was cooled to −15° C. under nitrogen. HCl gas was bubbled through for 15 min, and the reaction solution warmed to 0° C. for 2h. The solvent was removed in vacuo to provide the titled product.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06387903B1
Source datasetuspto-grants-2002_05
ORD IDord-a99e841a89df45269a172638b37d1ac1
Source noteuspto-grants-2002_05