HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 22464539, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 22464486 | HCID 22464486 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | HCID 22464539 | HCID 22464539 | — |
Reaction Steps
To a stirred solution of N-Boc-2-(2,2,2-trifluoroethylsulfonyl)benzylamine (480 mg) in dioxane (4.0 mL) at room temperature was added excess 4.0 M HCl in dioxane. The mixture was stirred until no starting material remained by TLC and was then concentrated in vacuo to afford the title compound as an off-white solid:
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06387911B1 |
| Source dataset | uspto-grants-2002_05 |
| ORD ID | ord-dbc7cc15fc644a0dba20bf2f118640ba |
| Source note | uspto-grants-2002_05 |