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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1935452Generated: November 1, 2026

Hydrochloric Acid → HCID 22464539, compound

https://huagongshe.com/reaction/1935452

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHydrochloric AcidHCID 313—
ReactantHCID 22464486HCID 22464486—
Solvent1,4-DioxaneHCID 31275—
ProductHCID 22464539HCID 22464539—

Reaction Steps

To a stirred solution of N-Boc-2-(2,2,2-trifluoroethylsulfonyl)benzylamine (480 mg) in dioxane (4.0 mL) at room temperature was added excess 4.0 M HCl in dioxane. The mixture was stirred until no starting material remained by TLC and was then concentrated in vacuo to afford the title compound as an off-white solid:

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06387911B1
Source datasetuspto-grants-2002_05
ORD IDord-dbc7cc15fc644a0dba20bf2f118640ba
Source noteuspto-grants-2002_05