HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzaldehyde → 2-Benzylidene-1-indanone
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzaldehyde | HCID 240 | — |
| Reactant | 1-Indanone | HCID 6735 | — |
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | 2-Benzylidene-1-indanone | HCID 288876 | — |
Reaction Steps
To a solution of 1-indanone (5.0 g) and benzaldehyde (4.1 g) in methanol (40 ml), was added 2.2 ml of 48% aqueous sodium hydroxide solution. The reaction mixture was stirred at room temperature for 0.5 hr. The resulting precipitate was filtered and washed with water. The yield was 7.9 g.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06388090B2 |
| Source dataset | uspto-grants-2002_05 |
| ORD ID | ord-e299c80eba01428bad09ea6dccf1ec79 |
| Source note | uspto-grants-2002_05 |