HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Fluoro-4-methoxyaniline → 2,3,4-Trifluoro-1-[(3-Fluoro-4-methoxyphenyl)aminosulfonyl]benzene
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Fluoro-4-methoxyaniline | HCID 581110 | — |
| Reactant | 2,3,4-Trifluorobenzenesulfonyl chloride | HCID 2776977 | — |
| Product | 2,3,4-Trifluoro-1-[(3-Fluoro-4-methoxyphenyl)aminosulfonyl]benzene | HCID 12016875 | — |
Reaction Steps
The title compound was prepared in a manner similar to that described in Example 1, by replacing 4-fluoro-3-nitrophenylsulfonyl chloride with 2,3,4-trifluorophenylsulfonyl chloride and replacing p-anisidine with 3-fluoro-4-methoxyaniline. 1H-NMR (CDCl3): δ 7.52 (1H, m), 7.00 (1H, m), 6.93 (1H, m), 6.80 (2H, m), 6.70 (1H, br s), 3.80 (3H, s).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06388131B2 |
| Source dataset | uspto-grants-2002_05 |
| ORD ID | ord-257e858b74b149049dacd207c4933253 |
| Source note | uspto-grants-2002_05 |