反应详情

A solution of 4.02 g (11.86 mmol) N-benzyl-6-(4-phenylbutoxy)hexylamine in 40 ml EtOH is hydrogenated at room temperature and atmospheric pressure with 0.4 g 5% Pd/C. When 300 ml H2 have been absorbed, the mixture is filtered on decalite and the filtrate is concentrated to yield 2.89 g (97.9%) 6-(4-phenylbutoxy)hexylamine as an oil.

1. customis hydrogenated at room temperature
2. customWhen 300 ml H2 have been absorbed
3. filtrationthe mixture is filtered on decalite
4. concentrationthe filtrate is concentrated