HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-benzyl-6-(4-phenylbutoxy)hexan-1-amine → 6-(4-Phenylbutoxy)hexan-1-amine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-benzyl-6-(4-phenylbutoxy)hexan-1-amine | HCID 10914757 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | 6-(4-Phenylbutoxy)hexan-1-amine | HCID 10966902 | 97.9% |
Reaction Steps
A solution of 4.02 g (11.86 mmol) N-benzyl-6-(4-phenylbutoxy)hexylamine in 40 ml EtOH is hydrogenated at room temperature and atmospheric pressure with 0.4 g 5% Pd/C. When 300 ml H2 have been absorbed, the mixture is filtered on decalite and the filtrate is concentrated to yield 2.89 g (97.9%) 6-(4-phenylbutoxy)hexylamine as an oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06388134B1 |
| Source dataset | uspto-grants-2002_05 |
| ORD ID | ord-f81998c366584b50bb1ceae388beb513 |
| Source note | uspto-grants-2002_05 |