HuagongsheHuagongshe Chemistry Print Report · For research reference only
Oxygen → HCID 12039381, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Oxygen | HCID 977 | — |
| Reactant | HCID 11209898 | HCID 11209898 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | HCID 12039381 | HCID 12039381 | — |
Reaction Steps
A mixture of 10 mmol of the obtained 1.3-di(t-butoxycarbonyl)adamantane, 2 mmol of NHPI, 0.1 mmol of acetylacetonatocobalt Co(AA)2, and 25 ml of acetic acid was stirred in an atmosphere of oxygen at 75° C. for 6 hours. As a result, there was obtained 1,3-di(t-butoxycarbonyl)-5-hydroxyadamantane.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06391520B1 |
| Source dataset | uspto-grants-2002_05 |
| ORD ID | ord-803503d2d2e6434088936d9325d3e78d |
| Source note | uspto-grants-2002_05 |