HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Hydrazino-delta-2-imidazoline hydrobromide → HCID 69536384, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Hydrazino-delta-2-imidazoline hydrobromide | HCID 3085099 | — |
| Reactant | 3-(4-Hydroxyphenyl)propanal | HCID 11957427 | — |
| Reactant | HCID 15857342 | HCID 15857342 | — |
| Product | HCID 69536384 | HCID 69536384 | 8.4% |
Reaction Steps
The operation is carried out as in Example 1 Stages A, B and C but using 190 mg of 3-(4-hydroxyphenyl)-propanal and 530 mg of ethyl 4-bromo-2-[[(phenylmethoxy)carbonyl]amino]butanoate (Stage A) then, during Sage B, 92 mg of 4,5-dihydro-1H-imidazol-2-yl-hydrazine hydrobromide. 20 mg of expected product is obtained in the form of an E/Z mixture 90/10.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06391904B1 |
| Source dataset | uspto-grants-2002_05 |
| ORD ID | ord-1297fa6957e84c208427efa3e1fe2ce6 |
| Source note | uspto-grants-2002_05 |