HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Hydroxide → HCID 86584189, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | HCID 70130482 | HCID 70130482 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 86584189 | HCID 86584189 | — |
Reaction Steps
To a solution of (2S)-1-[((6S)-3-ethoxycarbonylmethoxy-6,7,8,9-tetrahydro-5H-benzocyclohepten-6-yl)amino]-3-phenoxy-2-propanol (249 mg) in ethanol (1 ml) was added 1N sodium hydroxide at 5° C. After stirred at room temperature for 2 hours, the mixture was evaporated in vacuo to afford sodium [(6S)-6-[((2S)-2-hydroxy-3-phenoxypropyl)amino]-6,7,8,9-tetrahydro-5H-benzocyclohepten-3-yloxy]acetate (210 mg).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06391915B2 |
| Source dataset | uspto-grants-2002_05 |
| ORD ID | ord-7e0186dbfd86435394173dc2ef718fb8 |
| Source note | uspto-grants-2002_05 |