Magnesium → HCID 22462486, compound

HRID 1936992Notes

Reaction equation

HRID 1936992 reaction equation
[CH3:1][O:2][C:3]1[CH:12]=[CH:11][C:10]2[NH:9][C:8](=[O:13])[C:7]3[CH2:14][CH2:15][CH2:16][C:6]=3[C:5]=2[CH:4]=1.[Mg]>>[CH3:1][O:2][C:3]1[CH:12]=[CH:11][C:10]2[NH:9][C:8](=[O:13])[CH:7]3[CH2:14][CH2:15][CH2:16][CH:6]3[C:5]=2[CH:4]=1

Participants

3

Reactant 2

HCID 5462224MagnesiumHCID 22462468HCID 22462468, compound

Product 1

HCID 22462486HCID 22462486, compoundYield 10.2%

Procedure

8-Methoxy-1,2,3,5-tetrahydrocyclopenta[c]quinolin-4-one (0.78 g, 3.6 mmol) and magnesium (2.5 g, 103 mmol) are reacted to form 80 mg (10%) of product analogously to Example 7.

Sources & evidence

ORD record
ord-59aeef87c5d84429a662df81ab426750
Source dataset
uspto-grants-2002_05
Patent number
US06391887B1

Reaction notes

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