Magnesium → HCID 22462427, compound

HRID 1937011Notes

Reaction equation

[F:1][C:2]1[CH:3]=[CH:4][C:5]2[C:6]3[CH2:15][CH2:14][CH2:13][C:7]=3[C:8](=[O:12])[NH:9][C:10]=2[CH:11]=1.[Mg]>>[F:1][C:2]1[CH:3]=[CH:4][C:5]2[CH:6]3[CH2:15][CH2:14][CH2:13][CH:7]3[C:8](=[O:12])[NH:9][C:10]=2[CH:11]=1

Participants

Reactant 2

HCID 5462224Magnesium

HCID 22462493HCID 22462493, compound

Product 1

HCID 22462427HCID 22462427, compoundYield 17%

Procedure

7-Fluoro-1,2,3,5-tetrahydrocyclopenta[c]quinolin-4-one (1.0 g, 4.9 mmol) and magnesium (1.2 g, 49.2 mmol) are reacted to form 170 mg (17%) of product analogously to Example 7.

Sources & evidence

ORD record: ord-565909e1182642c191ff2e2710aa22eb
Source dataset: uspto-grants-2002_05
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US06391887B1

Reaction notes

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