HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methylamine → HCID 178482310, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methylamine | HCID 6329 | — |
| Reactant | HCID 10878248 | HCID 10878248 | — |
| Product | HCID 178482310 | HCID 178482310 | — |
Reaction Steps
1,2,3,3a,5,9b-Hexahydrocyclopenta[c]quinoline-4-thione (90 mg, 0.44 mmol) is stirred in 2 M methanolic methylamine solution (15 ml) for 24 hours at room temperature. After concentration by evaporation, the residue is purified on silica gel with dichloromethane-methanol: 90 mg (99%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06391887B1 |
| Source dataset | uspto-grants-2002_05 |
| ORD ID | ord-c25056f4c8ad42118f953227d84d7214 |
| Source note | uspto-grants-2002_05 |