Acetic Anhydride → HCID 70023899, compound

Participants

Reaction Steps

To a solution of (±)-3-(3-aminophenyl)-9-methyl-9-azabicyclo[3.3.1]non-2-ene (0.43 g, 1.9 mmol) in dichloromethane was added dropwise, Acetic Acid anhydride (0.25 g, 0.23 ml) at 0° C. The mixture was triturated with petroleum ether (2×10 ml), followed by diethyl ether (10 ml). Yield 0.34 g, 55%. Mp. 59.9-63.4° C.

Provenance & Evidence