4-Fluorobenzyl chloride → HCID 11447904, compound

Participants

Reaction Steps

In the same apparatus and procedure as Example 1 above, 0.20 g (0.68 mmol) of tetrabutylphosphonium chloride, 1.00 g (6.92 mmol) of 4-fluorobenzyl chloride, and 2.80 g (20.7 mmol) of trichlorosilane were reacted at 130° C. for 4 hrs. The resulting mixture was distilled to give 1.19 g of (4-fluorobenzyl)trichlorosilane (82%).

Provenance & Evidence