反应详情

A solution of 116 (0.27 g) in MeOH (10 mL) was treated with 0.135 M sodium methoxide (4.9 mL) in MeOH. After 4 h, the solvent was evaporated, the residue was suspended in H2O, and the solid was collected by filtration. The solid was crystallized from EtOAc-ether to give a tan powder, m.p. 206-208° C.

1. customthe solvent was evaporated
2. filtrationthe solid was collected by filtration
3. customThe solid was crystallized from EtOAc-ether
4. customto give a tan powder, m.p. 206-208° C.