HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 22461188, compound → HCID 9865125, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 22461188 | HCID 22461188 | — |
| Solvent | Hydrochloric Acid | HCID 313 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 9865125 | HCID 9865125 | 109.5% |
Reaction Steps
A solution of (±)-2-[3-(4-tert-butyl-2-methoxy-benzoylamino)-phenyl]-1-(tert-butyloxycarbonyl)-pyrrolidine (0.034 g) in methanol (3 mL) and 5M HCl (2 mL) was allowed to stir at room temperature for 18 h. Evaporation in vacuo gave the title compound as a colourless solid (0.029 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06395759B1 |
| Source dataset | uspto-grants-2002_05 |
| ORD ID | ord-f3bc319d5fcf4548afa567abfc6f7341 |
| Source note | uspto-grants-2002_05 |