HuagongsheHuagongshe Chemistry Print Report · For research reference only
Nitrobenzene → Naphtho[2,3-b]furan-4,9-dione, 8-hydroxy-2-methyl-
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Nitrobenzene | HCID 7416 | — |
| Reactant | 2-Acetyl-5-Methylfuran | HCID 14514 | — |
| Reactant | 3-Hydroxyphthalic anhydride | HCID 96580 | — |
| Reactant | Aluminum(III) Chloride | HCID 6451240 | — |
| Product | Naphtho[2,3-b]furan-4,9-dione, 8-hydroxy-2-methyl- | HCID 9794563 | — |
Reaction Conditions
| Temperature | 100 °C |
|---|
Reaction Steps
Aluminum chloride (2.5 g) and 3-hydroxyphthalic anhydride (1 g) were added to nitrobenzene (5 ml), to which was added 2-acetyl-5-methylfuran (0.7 g), dropwise, and heated at 100° C. overnight.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06395773B1 |
| Source dataset | uspto-grants-2002_05 |
| ORD ID | ord-e44b4be7438d4d5ba5f0ff216aba7041 |
| Source note | uspto-grants-2002_05 |