HuagongsheHuagongshe Chemistry Print Report · For research reference only
Pyridine → HCID 86583726, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Pyridine | HCID 1049 | — |
| Reactant | Oxalyl chloride | HCID 65578 | — |
| Reactant | HCID 86583727 | HCID 86583727 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 86583726 | HCID 86583726 | — |
Reaction Steps
Pyridine was added to a solution of pNB oxalylchloride in acetonitrile. After 20 minutes the TES azetidinone isobutyl carbonate was added. The reaction was given an aqueous work up, the organics were concentrated in vacuo to afford TES oxalimide isobutyl carbonate (15.2 g) as a white solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06395894B2 |
| Source dataset | uspto-grants-2002_05 |
| ORD ID | ord-a4063cc4a3c44028911bb8ab94781ef6 |
| Source note | uspto-grants-2002_05 |