Piperidine → HCID 178519853, compound

HRID 1937851Notes

Reaction equation

HRID 1937851 reaction equation
C1CCNCC1.O=C(c1c[nH]c2ccc(Br)cc12)[C@@H]1CCCN1C(=O)OCc1ccccc1>CC(C)(C)[O-].CC(C1=C(P(C2CCCCC2)C2CCCCC2)C=C[CH]1)P(C(C)(C)C)C(C)(C)C.COCCOC.[CH]1C=CC=C1.[Fe].[Na+]>O=C(c1c[nH]c2ccc(N3CCCCC3)cc12)[C@@H]1CCCN1C(=O)OCc1ccccc1

Participants

6

Reactant 2

HCID 8082PiperidineHCID 18661140HCID 18661140, compound

Product 1

HCID 178519853HCID 178519853, compoundYield 8%

Reagents, catalysts & solvents 3

HCID 23676156Sodium t-butoxideReagentHCID 178437370HCID 178437370, compoundCatalystHCID 80711,2-DimethoxyethaneSolvent2×

Conditions

Temperature
80 °C

Workup

  1. additionNo procedure recorded

Sources & evidence

ORD record
ord-6faf242952394924af60191965cee5b8
Source dataset
Pd_CN_Coupling_Informer_Library
Original link
View source

Reaction notes

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