Piperidine → HCID 178439936, compound

HRID 1937861Notes

Reaction equation

HRID 1937861 reaction equation
C1CCNCC1.CCCc1nc2ccc(I)cc2c(=O)n1Cc1ccc(-c2ccccc2S(=O)(=O)NC(C)(C)C)cc1>CC(C)(C)[O-].CC(C1=C(P(C2CCCCC2)C2CCCCC2)C=C[CH]1)P(C(C)(C)C)C(C)(C)C.COCCOC.[CH]1C=CC=C1.[Fe].[Na+]>CCCc1nc2ccc(N3CCCCC3)cc2c(=O)n1Cc1ccc(-c2ccccc2S(=O)(=O)NC(C)(C)C)cc1

Participants

6

Reactant 2

HCID 8082PiperidineHCID 132556033HCID 132556033, compound

Product 1

HCID 178439936HCID 178439936, compoundYield 20%

Reagents, catalysts & solvents 3

HCID 23676156Sodium t-butoxideReagentHCID 178437370HCID 178437370, compoundCatalystHCID 80711,2-DimethoxyethaneSolvent2×

Conditions

Temperature
80 °C

Workup

  1. additionNo procedure recorded

Sources & evidence

ORD record
ord-d3701ba305c14bc2a2dd6d69b3ba67ba
Source dataset
Pd_CN_Coupling_Informer_Library
Original link
View source

Reaction notes

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