Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
1-[4-(N,N-diethylaminosulfonyl)phenyl]-4,4,4-trifluoro-3-hydroxy-3-methylbut-1-yne → 1-[4-(N,N-Diethylaminosulfonyl)phenyl]-4,4,4-trifluoro-3-hydroxy-3-methyl-trans-but-1-ene
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 1-[4-(N,N-diethylaminosulfonyl)phenyl]-4,4,4-trifluoro-3-hydroxy-3-methylbut-1-yne | HCID 21469113 | — |
| 반응물 | 4,4,4-Trifluoro-3-hydroxy-3-methyl-1-[4-(1-pyrrolidinylsulfonyl)phenyl]but-1-yne | HCID 21469115 | — |
| 생성물 | 1-[4-(N,N-Diethylaminosulfonyl)phenyl]-4,4,4-trifluoro-3-hydroxy-3-methyl-trans-but-1-ene | HCID 21469122 | — |
반응 단계
Using a procedure similar to that described in Example 11, but substituting 1-[4-(N,N-diethylaminosulfonyl)phenyl]-4,4,4-trifluoro-3-hydroxy-3-methylbut-1-yne for the 4,4,4-trifluoro-3-hydroxy-3-methyl-1-[4-(1-pyrrolidinylsulfonyl)phenyl]but-1-yne used therein, the title compound was prepared; mp 112.1°-117.2° C.; MS: m/z=352(M+1). Analysis for C15 H20F3NO3S: Calculated: C, 51.27; H, 5.74; N, 3.99. Found: C, 51.17; H, 5.96; N, 3.87.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05693639 |
| 출처 데이터셋 | uspto-grants-1997_12 |
| ORD ID | ord-b2bd1c8683854b218668421b94cfcfd8 |
| 출처 메모 | uspto-grants-1997_12 |