HuagongsheHuagongshe Chemistry Print Report · For research reference only
Pyridinium chloride → HCID 21469456, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Pyridinium chloride | HCID 10176127 | — |
| Reactant | HCID 21469374 | HCID 21469374 | — |
| Solvent | Pyridine | HCID 1049 | — |
| Product | HCID 21469456 | HCID 21469456 | — |
Reaction Steps
A mixture of 1.6 g of 3-[1-(4-(indol-3-yl)butyl)-4-piperidyl]-5-methoxyindole [which can be prepared according to Example 1], 1.8 g of pyridine hydrochloride and 50 ml of pyridine is boiled for 3 hours. The mixture is cooled, the solvent is evaporated and the residue is worked up in a conventional manner and gives 3-[1-(4-(indol-3-yl)butyl)-4-piperidyl]-5-hydroxyindole, m.p. 178°-180°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05693655 |
| Source dataset | uspto-grants-1997_12 |
| ORD ID | ord-c1c3eea670ba445297e6d60b6241975e |
| Source note | uspto-grants-1997_12 |