HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 21469388, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Methanol | HCID 887 | — |
| Reactant | HCID 21469386 | HCID 21469386 | — |
| Product | HCID 21469388 | HCID 21469388 | — |
Reaction Steps
HCl gas is passed into a boiling solution of 2.5 g of 3-[1-(4-(5-carboxyindol-3-yl)butyl)-4-piperidyl]-5-fluoroindole in 50 ml of absolute methanol for hours. The mixture is then boiled for a further hour, is worked up in a conventional manner and gives 3-[1-(4-(5-methoxycarbonylindol-3-yl)butyl)-4-piperidyl]-5-fluoroindole.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05693655 |
| Source dataset | uspto-grants-1997_12 |
| ORD ID | ord-9e1a4a2227824166b3fff6f268d374a4 |
| Source note | uspto-grants-1997_12 |