反应详情

A mixture of 3-trimethylsilyltoluene (3.28 g, 10 mmol), N-bromosuccinimide (1.78 g, 10 mmol) and benzoylperoxide (10 mg) in CCl4 (20 ml) was stirred under reflux for 3 hours, then cooled and filtered. The solvent was removed under reduced pressure and 3-trimethylsilylbenzylbromide was purified by distillation.

1. temperatureunder reflux for 3 hours
2. temperaturecooled
3. filtrationfiltered
4. customThe solvent was removed under reduced pressure and 3-trimethylsilylbenzylbromide
5. distillationwas purified by distillation