HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → HCID 21469488, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | 1-Bromododecane | HCID 8919 | — |
| Reactant | HCID 178509541 | HCID 178509541 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 21469488 | HCID 21469488 | — |
Reaction Steps
The tetrazole (b) obtained above (11.0 g; 0.067 moles) was dissolved in acetonitrile (150 mL) containing one equivalent of triethylamine (6.8 g; 0.067 moles). The solution was heated to reflux followed by the addition of 1-bromo dodecane (16.8 g; 0.067 moles). Isolation of the 2-isomer was achieved employing the same conditions described for Example 11.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05693657 |
| Source dataset | uspto-grants-1997_12 |
| ORD ID | ord-c2fb38bb1ea34cfe96948421103ff4c5 |
| Source note | uspto-grants-1997_12 |