HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → 3-Methylfuran-2-carbonyl chloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | 3-Methyl-2-furoic acid | HCID 78127 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | 3-Methylfuran-2-carbonyl chloride | HCID 2796674 | — |
Reaction Steps
3-Methyl-2-furancarbonyl chloride was prepared by refluxing 3-methyl-2-furancarboxylic acid (20.0 g) with thionyl chloride (25 ml) in toluene (75 ml) for 3 hours. After removal of the solvent, the acid chloride was distilled (b.p. 74°-76° C. at ca. 12 mm).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05693827 |
| Source dataset | uspto-grants-1997_12 |
| ORD ID | ord-f64822d702a043b690ce1a55d07162f8 |
| Source note | uspto-grants-1997_12 |