HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonia → N-(3,4,4-trifluoro-3-butenyl)ethanediamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonia | HCID 222 | — |
| Reactant | Oxo[(3,4,4-trifluoro-3-butenyl)amino]oxoacetic acid, methyl ester | HCID 86748464 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | N-(3,4,4-trifluoro-3-butenyl)ethanediamide | HCID 15239196 | 68% |
Reaction Steps
A solution of Compound 142 (5.0 g, 0.0237 mole) in methanol (50 mL) is saturated with dry gaseous ammonia at room temperature. The precipitate is filtered, washed with methanol and dried to give 3.16 g of the title compound as a white solid, a 68% yield. m.p. 190°-220° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05693865 |
| Source dataset | uspto-grants-1997_12 |
| ORD ID | ord-e4325b4767114a76b0a8e7feac1d924a |
| Source note | uspto-grants-1997_12 |