Potassium Carbonate → HCID 21223274, compound

HRID 1939148Notes

Reaction equation

HRID 1939148 reaction equation
C([O:4][CH2:5][C:6]1[O:11][C:10]([CH3:13])([CH3:12])[O:9][C:8](=[O:14])[C:7]=1[C:15]1[CH:20]=[CH:19][CH:18]=[CH:17][CH:16]=1)(=O)C.C(=O)([O-])[O-].[K+].[K+]>CO>[OH:4][CH2:5][C:6]1[O:11][C:10]([CH3:12])([CH3:13])[O:9][C:8](=[O:14])[C:7]=1[C:15]1[CH:16]=[CH:17][CH:18]=[CH:19][CH:20]=1

Participants

4

Reactant 2

HCID 11430Potassium CarbonateHCID 15405501HCID 15405501, compound

Product 1

HCID 21223274HCID 21223274, compound

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent

Procedure

6-Acetyloxymethyl-2,2-dimethyl-5-phenyl-2H,4H-1,3-dioxin-4-one (Compound No. 241, 7.46 g) was dissolved in methanol (108 ml), and cooled with ice; then, an aqueous solution (27 ml) of potassium carbonate (2.42 g) was added slowly thereto.

Workup

  1. temperaturecooled with ice

Sources & evidence

ORD record
ord-4ac8c0494692407ca389b859d592387d
Source dataset
uspto-grants-1997_12
Patent number
US05696054

Reaction notes

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