反应详情

As described for Example 1, 4-(4-aminobenzoyl)-5,6,7,8-tetrahydro-4H-thieno[3,2-b]azepine (0.001 ml) is reacted with 2-methylbenzoyl chloride in dichloromethane to give the product. Crystallization from ethyl acetate-hexane gives crystals, m.p. 181°-182° C.

1. customto give the product
2. customCrystallization from ethyl acetate-hexane
3. customgives crystals, m.p. 181°-182° C.