HuagongsheHuagongshe Chemistry Print Report · For research reference only
alpha-Naphthyl isocyanate → HCID 23209071, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | alpha-Naphthyl isocyanate | HCID 66589 | — |
| Reactant | 2-Amino-4-(trifluoromethyl)phenol | HCID 120246 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 23209071 | HCID 23209071 | 72% |
Reaction Steps
2-hydroxy-5-(trifluoromethyl)aniline (0.12 g, 0.7 mmol) in toluene (3 ml) was added to a solution of alpha-naphthyl isocyanate (0.11 g, 0.7 mmol) in toluene (3 ml). The reaction was stirred at RT overnight and the product filtered off. 0.17 g (72%) of the title compound was isolated. M.p. 205°-207° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05696138 |
| Source dataset | uspto-grants-1997_12 |
| ORD ID | ord-10d93b7cf48a4e8686b7545bf140e9d0 |
| Source note | uspto-grants-1997_12 |