HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanone, (3-aminophenyl)phenyl- → N-(3-benzoylphenyl)-N'-(2-methoxy-5-chlorophenyl) urea
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanone, (3-aminophenyl)phenyl- | HCID 17817 | — |
| Reactant | 4-Chloro-2-isocyanato-1-methoxybenzene | HCID 144009 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | N-(3-benzoylphenyl)-N'-(2-methoxy-5-chlorophenyl) urea | HCID 53686550 | 92.4% |
Reaction Steps
A mixture of 5-chloro-2-methoxyphenyl isocyanate (1.00 g, 5.4 mmol) and 3-aminobenzophenone (1.29 g, 6.5 mmol) was stirred in toluene (20 ml) for two days. The reaction was filtered and the filter cake washed with toluene. 1.9 g of the title compound was isolated.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05696138 |
| Source dataset | uspto-grants-1997_12 |
| ORD ID | ord-cd922a6dd0144ddf8addaae32b83b2f4 |
| Source note | uspto-grants-1997_12 |