Hydrochloric Acid → HCID 131720352, compound

HRID 1939408Notes

Reaction equation

HRID 1939408 reaction equation
[NH2:1][C:2]([NH2:24])=[N:3][C:4](=[O:23])[C:5]1[CH:10]=[C:9]([S:11]([CH3:14])(=[O:13])=[O:12])[C:8]([S:15][C:16]2[CH:21]=[CH:20][N:19]=[CH:18][CH:17]=2)=[CH:7][C:6]=1[CH3:22].[ClH:25]>O>[ClH:25].[ClH:25].[NH2:24][C:2]([NH2:1])=[N:3][C:4](=[O:23])[C:5]1[CH:10]=[C:9]([S:11]([CH3:14])(=[O:13])=[O:12])[C:8]([S:15][C:16]2[CH:21]=[CH:20][N:19]=[CH:18][CH:17]=2)=[CH:7][C:6]=1[CH3:22]

Participants

4

Reactant 2

HCID 313Hydrochloric AcidHCID 9950952HCID 9950952, compound

Product 1

HCID 131720352HCID 131720352, compound

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Procedure

0.9 g of N-diaminomethylene-2-methyl-4-(4-pyridylthio)-5-methylsulfonylbenzamide [obtainable in accordance with Example 1] is suspended in 100 ml of H2O and dissolved with 1 molar aqueous HCl solution and the solution is then freeze-dried, to give N-diaminomethylene-2-methyl-4-(4-pyridylthio)-5-methylsulfonylbenzamide, dihydrochloride, m.p.>250°.

Workup

  1. customthe solution is then freeze-dried

Sources & evidence

ORD record
ord-423f77016c964a41ba82287091db836a
Source dataset
uspto-grants-1997_12
Patent number
US05696167

Reaction notes

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