HCID 18349474, compound → 4-Methoxyphenyl 5,6-dihydroxyhexyl ether

Participants

Reaction Steps

2.08 g of 4-methoxyphenyl 4-(2,2-dimethyldioxolan-4-yl)butyl ether from Example 1b were dissolved in 165 ml of 80% acetic acid and stirred at room temperature for 4 h. The acetic acid was separated off in vacuo, and the mixture was then coevaporated with toluene/methanol twice. This resulted in a crystalline product.

Provenance & Evidence