O-Xylene → Zinc 2-ethylhexoate

Participants

Reaction Steps

A liquid zinc oxide precursor solution was prepared by mixing zinc 2-ethylhexanoate into a 50/50 (v/v) solvent mixture of xylene and butyl acetate to provide a zinc 2-ethylhexanoate concentration of about 0.1 mol/L. Bismuth 2-ethylhexanoate was added to this mixture under a desiccated atmosphere having less than about 40% humidity in a quantity sufficient to produce bismuth concentrations of 0, 0.5, 1, and 5 mole percent bismuth 2-ethylhexanoate. These bismuth concentrations were determined as the number of moles of bismuth 2-ethylhexanoate divided by the number of moles of bismuth 2-ethylhexanoate plus the number of moles of zinc 2-ethylhexanoate, i.e, bismuth as a percentage of total metals.

Provenance & Evidence