HuagongsheHuagongshe Chemistry Print Report · For research reference only
Cesium carbonate → HCID 15341379, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Cesium carbonate | HCID 10796 | — |
| Reactant | Sesamol | HCID 68289 | — |
| Reactant | HCID 21462919 | HCID 21462919 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 15341379 | HCID 15341379 | — |
Reaction Steps
A solution of 3.8 g of ethyl 4-(1,4-benzodioxan-6-yl)-2-chlorobenzofuro[3,2-b]pyridine-3-carboxylate and 3.1 g of caesium carbonate in 40 ml of DMF is treated with a solution of 1.7 g of 3,4-methylenedioxyphenol in 20 ml of dichloromethane and stirred overnight. The mixture is worked up in the customary manner and ethyl 4-(1,4-benzodioxan-6-yl)-2-(3,4-methylenedioxyphenoxy)benzofuro[3,2-b]pyridine-3-carboxylate is obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05700807 |
| Source dataset | uspto-grants-1997_12 |
| ORD ID | ord-3ad438d9867f4edfb9cfc41eacb51de7 |
| Source note | uspto-grants-1997_12 |