HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 21463514, compound → HCID 21463565, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 21463514 | HCID 21463514 | — |
| Reactant | HCID 56997307 | HCID 56997307 | — |
| Product | HCID 21463565 | HCID 21463565 | 20% |
Reaction Steps
The procedure of Example 22-i) was repeated using 1,3-biscyanomethyl-2-chlorobenzene (870 mg, 4.4 mmol) and 2-amino-3,4-difluorothiophenol hydrochloride (956 mg, 4.8 mmol) and the resultant product was recrystallized from ethyl acetate-hexane to give 3-[(4,5-difluorobenzothiazol-2-yl)methyl]-2-chlorophenylacetonitrile (295 mg, 20%) as a colorless powder.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05700819 |
| Source dataset | uspto-grants-1997_12 |
| ORD ID | ord-d0f94fb21e6640ef99944bd8beba35a5 |
| Source note | uspto-grants-1997_12 |