HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-(6-Methoxy-2-naphthyl)propionic acid → 2-(6-methoxynaphthalen-2-yl)propanoyl Chloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-(6-Methoxy-2-naphthyl)propionic acid | HCID 1302 | — |
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Solvent | Chloroform | HCID 6212 | — |
| Product | 2-(6-methoxynaphthalen-2-yl)propanoyl Chloride | HCID 10198829 | — |
Reaction Steps
7 ml of thionyl chloride were cautiously added to a solution of 2.3 g of 2-(6-methoxy-2-naphtyl)propionic acid in 15 ml of anhydrous chloroform. The reaction mixture was stirred for 40 minutes at room temperature and then the solvent was evaporated at a reduced pressure, obtaining 2.23 g of 2-(6-methoxy-2-naphtyl)propionylchloride.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05700947 |
| Source dataset | uspto-grants-1997_12 |
| ORD ID | ord-942f26f0325747ce85a01583f535b866 |
| Source note | uspto-grants-1997_12 |